Carbasalate calcium/Carbaspirin calcium

CAS number: 5749-67-7

Molecular formula: C₁₉H₁₈CaN₂O₉

molecular weight: 458.064

Chemical structure:

Testing ItemsTesting Specifications Testing Results
AppearanceWhite or off-white, crystalline powder.White, crystalline
IdentificationA. Absorption maxima at 228nm and 276nm,
specify absorbance should be 363 to 379 at
 228nm and 49 to 53 at 276nm.
Complies
B. Infrared spectrum should correspond
to reference spectrum of Carbasalate Calcium
C. The solution gives reaction of Salicylates
D. Heat sample with sodium hydroxide, a colour
yellow or yellowish-brown,is produced and the
vapour turns red litmus paper blue.
E. It gives the reaction of Calcium
Appearance of SolutionColourless or not more opalescent than reference
suspension II .
Complies
Related substancesImpurity C should not more than 0.5%0.34%
Impurity B should not more than 0.15%0.01%
Any unspecified impurities should not more than 0.05%LTDL
Total impurities should not more than 0.7%0.35%
Heavy MetalsNot more than 10ppmComplies
WaterShould not more than 0.1%0.04%
AssayContain Carbasalate Calcium 99.0%-101.0%
calculated on the anhydrous basis.
100.10%